Effect of annealing atmosphere on the structure and dielectric properties of unfilled tungsten bronze ceramics Ba4PrFe0.5Nb9.5O30

Unfilled tungsten bronze ceramics with the nominal formula Ba₄PrFe_0.5Nb_9.5O₃₀ were synthesized via the standard solid-state sintering route, and the effects of oxygen vacancies on the dielectric and electrical properties were investigated in addition to the structure. Room-temperature X-ray diffraction showed that the N₂-annealed sample had the largest cell volume. Low-temperature spectrum showed that N₂ annealing rendered the dielectric constant and dielectric loss more frequency dispersive, whereas O₂ annealing inhibited the frequency dispersion. The dc conductivity of all the samples originated from the electrons produced in the second ionization of oxygen vacancies and was most likely controlled by a mixed conduction mechanism of the electron and oxygen-vacancy ions. The N₂-annealed sample has the highest dc conductivity owing to its high concentration of oxygen vacancies. The broadening of the Raman lines and the decrease of Raman intensity for the N₂-annealed sample originated from a significant structural disorder. X-ray photoelectron spectra demonstrated that the increased oxygen vacancies caused by the change of valences of Fe and Pr ions contributed to the structural disorder.     

Advanced Functional Materials Constructed from Pillar[n]arenes

Pillar[n]arenes are new generation of supramolecular macrocyclic host, which exhibit excellent host−guest recognition properties. In the last decade, functional materials constructed from pillar[n]arenes have been attracted more and more attention and displayed outstanding characteristics, such as stimuli-responsiveness, self-healing and adaptability. In this mini-review, we provide a survey of the pillar[n]arene-based literatures covering light-harvesting systems, functional hydrogels, and solid materials. It is anticipated that more and more pillar[n]arenes-based advanced materials with multi-functional properties will appear in the near future.     

薄膜铂电阻元件稳定性测试与分析

高端军事应用环境对测温传感器提出了小结构、高精度、良好的长期稳定性等要求,采用溅射方式制备的薄膜铂电阻元件成为了首选。通过分析薄膜铂电阻元件的结构、工艺,探讨影响稳定性的主要因素,包括薄膜缺陷、杂质、电迁移、结构封装应用与温度应力等。选择薄膜铂电阻在水三相点下的电阻值作为稳定性的比较基准,设计了一款不大于3mK的高精度测试系统。通过对薄膜铂电阻元件进行高温电寿命试验和温度冲击试验,评估得出薄膜铂电阻元件长期稳定性达到10mK,满足设计需求。     

Microwave bandpass filter by feedback interference topology

This paper proposes a signal feedback interference topology to control the characteristics of a coupled line bandpass filter. Control is carried out by varying the ratio of the transmission line parameters of the forward and the feedback couplers. The topology produces a compact filter that does not require a complicated design or fabrication. The results of the insertion and return losses show that the feedback‐controlled design has desirable features in terms of the design frequency, fractional bandwidth, stopband rejection level, roll‐off rate and insertion loss. The test results of the fabricated prototype achieved good agreement with the simulation results of the ideal transmission line design model. Several microwave, modern wireless and mobile/satellite communication systems may benefit from such a filter design due to its compactness and flexibility.     

矿用直线振动筛结构故障分析

针对煤矿选煤厂直线振动筛工作过程中出现的结构故障问题,采用有限元仿真与现场测试结合的方法对振动筛出现故障的原因进行了分析研究。介绍了振动筛的主要结构及常见故障,并以某矿选煤厂发生大梁断裂的振动筛为例,对该振动筛进行三维建模和有限元模态分析,分析结果表明:随着模态阶次的增加,振型的变化逐渐由移动转为结构本身的扭曲变形。在该振动筛空载工作状态下,选用本质安全型便携式测振记录仪进行振动测试并处理测试信号,得到该振动筛的工作频率。结合模态分析结果和实际测试结果,判断出空载时频繁运行振动筛是造成其大梁断裂的主要原因。根据故障原因给出维护建议:应当尽量避免振动筛在空载或物料较少的状态下长时间运行;在振动筛投入使用前,应预先了解振动筛的工作状态及可能存在的薄弱环节,尽可能避免结构故障,保证振动筛可靠运行。     

高泉背斜地层压力测井多参数综合解释与异常高压成因

目前国内外地层压力测井解释方法较多,但大多数方法基于欠压实沉积理论并局限于单一的地层岩性,尤其是针对盆地边缘山前深层构造,单一测井参数确定地层压力误差较大,且无法解释沉积压实机制以外的异常高压。为此,将多种异常高压机制相关的测井参数进行综合解释,建立适合山前复杂构造的地层压力测井多参数计算模型,评价准噶尔盆地南缘高泉背斜高探1井的地层压力剖面,其计算结果与钻井实测数据吻合,相对误差小于3.00%.同时,基于原始沉积加载—卸载过程力学原理,利用地层压力测井多参数分析判别出高泉背斜深层各层系异常高压的形成机制。     

脉冲高度权重技术测量197Au中子俘获截面

脉冲高度权重技术是利用C_6D_6探测器测量中子俘获截面的一种数据处理方法。在中国散裂中子源(China Spallation Neutron Source,CSNS)的反角白光中子源(Back-n)靶站上,通过测量金靶(~(197)Au)的中子俘获截面,验证了该方法的可靠性。首先利用Geant4蒙特卡罗程序模拟给出了不同靶条件下的探测器效率,脉冲高度权重函数等基本项,使得加权后的探测器效率与γ能量成正比。然后通过实验测量了~(197)Au中子俘获截面。结果表明:测量获得的中子俘获截面数据和ENDF/B-VⅢ.0评价数据相符合,同时发现随着实验靶尺寸的不同和质子束功率的增加,会使得实验本底的扣除误差越来越大。     

乌鲁木齐机场多普勒天气雷达故障统计分析

文章针对乌鲁木齐机场多普勒天气雷达(以下简称ADWR)2009~2019年发生的故障次数、故障分布以及备件更换情况,逐年统计故障率,深入分析了ADWR系统性能,总结出运行维护中的经验,就如何更好地提高雷达业务运行指标提出建议,以提高ADWR雷达的维护、维修能力,建立有针对性的备件管理,为科学的业务运行管理提供依据。